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TEK - Help With Extraction

Discussion in 'Peyote & San Pedro' started by rza, Oct 29, 2008.

  1. rza

    rza

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    swim has some san pedro and naOH and MEK was wondering if i could do a extraction with that.
     
  2. Dave_the_stoner

    Dave_the_stoner Titanium Member

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    I've seen a thread of using MEK over at wetdreams, but there were other chemicals needed.
     
  3. rza

    rza

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    really. excellent, where abouts?
     
  4. pistol pete

    pistol pete Silver Member

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    you could do just a simple extraction with iso alcohol or high proof ethanol, it will not be anywhere near pure obviously but u get a pea sized chunk of resin per trip.
    their is also an easy water,xyelene ,sodium hryoxide extractions that make it very close to pure, u keep some of the alkatiods from the cactis though, which swim doesnt mind. they add a nice effect. and it only takes about a day or so, longer sometimes due to evaporation. Swim could post the tek if ud like.
     
  5. Dave_the_stoner

    Dave_the_stoner Titanium Member

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    Heres what I was talking about, it's the only TEK I've seen using MEK (I'm sure theres gotta be other write ups using it somewhere on the web).
    http://www.wetdreams.ws/forum/topic.asp?TOPIC_ID=3566
    That crazy SOB SWIM has been contemplating between several TEKs to extract mescaline lately. He thinks Ekstaza's TEK is probably the best way to go.
     
  6. rza

    rza

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    every time i open it , it says
    Microsoft JET Database Engine error '80004005'
    Unspecified error
    /forum/inc_ipgate.asp, line 50
    ???
     
  7. 3rd_high

    3rd_high Silver Member

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    Same here
     
  8. Dave_the_stoner

    Dave_the_stoner Titanium Member

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    Ok sorry, I just logged out of there and it didnt let me view anything in thier forum, so I guess you have to be logged in to an account there to view anything so I'll copy/paste the bulk of it, I am doing so without permission from the author, so If he/she gets pissed off then they can direct any complaints to me (which I find unlikely, why would you do such a write up if not to share the knowlege?).

    this work was a collaboration between swim and one of his collegues...

    Approximately 3 grams of naturally occurring white mescaline HCl that had been previously produced by gassing an acetone spiked xylene freebase solution was added to 150 ml of boiling methyl ethyl ketone. The ketone was allowed to boil vigorously but was observed to be clouded by undissolved material. Distilled water was added by dropwise addition until the clouding cleared. The material was boiled down until the solvent just began to display signs of saturation, at which time, it was removed from the heat, covered and transferred to a freezer. At the conclusion of two hours time, the beaker was removed from the freezer and observed to be filled with a golden colored liquid saturated by a massive conglomeration of a material that bore uncanny resemblance to sparkling clean crushed ice. The contents of the beaker were fast filtered through a vacuum funnel and rinsed with very anhydrous ice cold mek followed ice cold anhydrous acetone. After subsequently stripping any residual solvent under vacuum, the material was observed to display spectacular clear needle formations, each roughly .10 mm in length.

    [​IMG]
    mescaline HCl grown from mek

    The bulk of this material was subsequently dissolved in a minimum of boiling distilled water and the volume of the solution reduced to just above saturation. At this time, the beaker was removed from the heat and placed on the lab bench for observation. It was immediately noticed that a thin skin of crystals had appeared around the upper interface between the walls of the beaker and the mescaline liquor. Within seconds, the skin began to expand radially inward at a rate of very roughly .2 mm/sec. Simultaneous to the skin moving across the surface of the liquid, an amazing array of fractal patterns appeared in its wake, frozen in the crystal. After an hour, the beaker was observed to be filled with long dagger shaped crystals that lay parallel to the base of the vessel. It was then flooded with anhydrous acetone and the crystals broken free into a suitable vacuum funnel. Upon drying under vacuum, the material assumed the appearance of very large white/clear shards of mescaline hydrochloride.

    [​IMG]
    mescaline HCl "shards" grown from water

    yes, the mek boil does for mescaline what it does for pseudo and meth!

    Close up of a cylinder of mescaline crashing out of mek... the dots of color are not digital artifacts as might be assumed, rather they are points of light reflecting off of the millions of crystal faces inside the cylinder.

    [​IMG]

    This is the "crude" material! It is what was collected out of the mek.

    [​IMG]

    The "crude" material above still had a hint of color to it, so we recrystalized it again from water. The following sequence shows how the shards grew in the mother liquour. Notice the patterns in the crystal.

    [​IMG]

    [​IMG]

    [​IMG]


    This is how it looked when it was finished. The remaining liquid is mostly acetone.

    [​IMG]


    After breaking the crystals free of the beaker, rinsing them with cold anhydrous mek and drying them, this is how they looked:

    [​IMG]


    written after being on the stuff for about 16 hours...

    Quote: she’s flabbergasted and stunned into a state of utter speechlessness.

    time and time and time again, she’s said that pure mescaline HCl in crystalline form is better than powder of any stripe…

    the drug she consumed last night was the strongest hallucinogen she’s ever used. She cannot begin to recall all the times she’s tripped on mescaline.

    this batch is Special.

    all these hours later… she’s still tripping. how long now? 16 hours, maybe?

    its going to last a full 24.

    it was smooth as the glass in which we constructed the Matrix… utter absence of body load (except the yummy parts…)… it was pure mind and soul… 100% immersion into the

    One.

    color. mescaline is the most colorful of all drugs except possibly dmt.

    somewhere near the peak, she took two massive rips off the DMT bong. She puked a little but barely remember it.

    the two most colorful of hallucinogens… the one with the shortest duration and one of the marathon duration drugs..

    they meshed seamlessly, each contributing it own characteristic color but combining to create something Unique.

    the mescaline pipe.

    this is how you extend the stuff indefinitely.

    in order to truly appreciate what the pipe has to offer, one must already be on the drug to begin with.

    when you are already tripping balls and you hit that pipe, it hits you just exactly the way DMT does… total immersion into hyperspace…

    only this is mescaline hyperspace, not dmtspace. it is as sudden and as vivid as DMT only it is mescaline at Warp 12.

    it becomes like crack.

    PedroCrack.

    but unlike cocaine, this stuff lasts for ages.

    if you hit that pipe every so often… every 4 hours or so… you never have to come down. no data on tolerance yet…

    she needs to come down but this is sooooo good.
    so swim finally passed out around 5 yesterday afternoon. Swim was still tripping then but did go to sleep. When swim woke up this morning, he was down. This stuff is just insanely potent.

    Swim did 500 mg, 140 mg intravenously and the remainder rectally.

    Swim doesn’t have entirely good data on the threshold dose as he had problems injecting the stuff. It was mixed at 700mg/gram --- just shy of the saturation point of the drug. The material was very thick and his vein withdrew from the needle as soon as the drug began to hit. By this time, he was tripping so hard that swim could no longer operate the syringe. He could no longer see clearly, so in the interest of his own safety, he aborted the remainder of the injection, broke the needle off and put the remainder of the shot up his ass. Within 20 minutes, he was tripping harder than the peak of previous mescaline experiences.

    The guys who took theirs orally reported that it began kicking in within ten minutes of using it.

    The shit behaved the same as crude mescaline in that it came in waves only the magnitude of psychedelic immersion was many orders of magnitude greater than anything swim has experienced with mescaline previously. It was almost as intense as DMT at the peak.

    yes, and DMT and mescaline mesh perfectly. The DMT made swim puke after the second massive rip off the bong but SWIM barely remember it.

    smoking mescaline works. But like swim said yesterday, it doesnt give you the full expereince unless you are already on the stuff.

    mek crystalization is the way to go with this drug. Those who fail to make use of this technique are going to rob themselves of the opportunity to experience mescaline full strength.

    the drug we are in possession of is not even the same shit as normal brown/tan mescaline HCl.

    this stuff is better than LSD. lasts much longer without having to be extended by amphetamines. it is very nearly as strong (in terms of how far out there it takes you...) as DMT.

    its easy to make. boil your crude in mek. shove it in the freezer. collect crystals. thats all there is to it.

    everyone complains about how hard it is to find LSD. who needs it??? this shit is better and we do not need a criminal organization to dole the stuff out to us for profit when and where they see fit to show up and collect our money.

    ANYONE can make the same stuff that we made with a minimum of effort.

    Here is another sequence showing the second pass (first was mek) growth of mescaline HCl crystals from water. Notice how some of the crystals are covered in zig-zag shaped markings across their faces... these are caused by impurities.

    [​IMG]

    [​IMG]

    [​IMG]

    [​IMG]

    [​IMG]


    amazingly, none of these represent the nicest crystals of all... swim also has clear as glass needles, some well over an inch long growing in IPA/mek/acetone/trace of water... these have been growing for days but are not finished yet. stay tuned. [​IMG]
     
    Last edited: Nov 1, 2008
  9. rza

    rza

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    so get pedro powder in jar with MEK and boil then put in fridge and u have pedro crack?

    rza added 900 Minutes and 23 Seconds later...

    could swim do this on some of his extract from alcohol?
     
    Last edited: Nov 14, 2008
  10. Captain Caveman

    Captain Caveman

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    What is MEK?

    Captain Caveman added 4 Minutes and 49 Seconds later...

    Swim does not understand that tek, why turn mescaline hcl, into mescaline hcl?

    The tek says at the start add 3 gram of natural white mescaline hcl

    Is this a way of making mescaline crack so to speak.
     
    Last edited: Nov 14, 2008
  11. rza

    rza

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    methyl ethyl ketone a paint thinner, and swim not sure either swim wants to know if you can do this with mescaline carbonate? or use MEK in a alcohol extraction?

    rza added 13 Minutes and 15 Seconds later...

    sounds good can swim use MEK instead of Xylene?
     
    Last edited: Nov 17, 2008
  12. Dave_the_stoner

    Dave_the_stoner Titanium Member

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    Basically thats just a further step after a good extraction to futher clean, and form it into big chunky crystals. Ive seen pictures of clear crystals using a gassing TEK, but this is the nicest I've has seen using solvents, of course I've only started looking at mescaline TEKS a couple months now.
    I havent seen any TEKs using MEK in place of xylene, but I'll post one if I encounter one. Toulene or naptha can be used in place of Xylene from What I've read, that may be easier to find.
     
    Last edited: Nov 18, 2008