Discussion in 'DMT and Ayahuasca' started by katukulysm, Nov 16, 2005.

  1. katukulysm

    katukulysm Mercury Member

    Reputation Points:
    Feb 14, 2005
    from U.S.A.
    wadda you think???&nbs p;&nbs p;

    How To Make DMT

    DMT stands for N,N-dimethyltryptamine. It is a semisynthetic
    compound similar to psilocin(the hallucinogenic substance in
    psilocybin) ins structure. The most common method of ingestion is
    smoking. Soaked parsley leaves are the usual method of ingestion
    although persons have dipped marijuana in it and said the
    experience was fantastic. The following recipe can be performed in
    the kitchen.

    Recipe for DMT:

    1. Mix thoroughly and dissolve 25 grams of indole with a pound of
    dry ethyl ether in a 2000 ml flask(2 quart jar.)

    2. Take an ice tray and fill with chipped or shaved ice. Cool
    solution for about 35 minutes until it reaches 0 degrees C. At the
    same time cool 50 ml dry oxalychloride to about 5 degrees below 0
    C. in the same ice tray.

    3. VERY slowly add the oxalychloride solution to the indole
    solution. These two chemicals are highly reactive. Avoid boiling
    over, contact with skin, and fumes.

    4. Wait until all the bubbling has died down, then add a few
    handfuls of table salt to the ice tray, to cool the solution
    further. Label the solution "solution 1" and put it in the

    5. Cool 100 ml. of dry ethyl ether in a 500 ml. flask to 0 degrees
    C. in a salted ice tray. At the same time cool an unopened bottle
    of dimethylamine to 0 degrees C. in the same ice bath.

    6. Open the seal of the dimethylamine bottle and slowly pour a
    steady stream into the ether. Label "solution 2."

    7. Very slowly and carefully add solution "1" and "2" together.

    8. Now take the mixed solutions from the ice tray and bring up to
    room temperature stirring the solution all the time. You should be
    left with a solution that is almost clear. If it is still murky,
    continue stirring until it becomes as clear as possible.

    9. Now filter the solution to seperate the precipitate by suction.

    <---Solution and Precipitate
    \ /<---Funnel / / <-- Rubber hose to
    \ / and / / Vacuum source
    \ / Filter/____/
    \*****\ /*************{ }*****/ <--- Two hole
    \****{ }*************{ }****/ rubber stopper
    \ { }&nbsp ; { } <-/--- Glass Tube
    \ { }&nbsp ; { } /
    | { }&nbsp ; { } |
    | |
    | |
    | |
    | |
    Figure A.

    10. Refilter with suction after pouring technical ether over the

    11. Repeat filtering once more with ether, then twice with water.

    12. Let this substance dry on a plastic or china plate.(do not use
    metal) After drying, a solid material will be formed. Take
    particles and place them in an 800 ml beaker.

    13. Mix 100 ml. benzene with 100 ml. methyl alcohol. After this
    mixture has been stirred, cover solid particles from step 12 with
    about 1/2 inch of the solution and heat the beaker in water until
    all solid material had dissolved. Add more solvent if
    necessary.(Note: Do not place beaker in water bath directly over
    the flame.)

    14. After all solid material has dissolved, remove beaker from the
    heat, and allow to cool. As it cools, small needle-shaped crystals
    will appear. When this happens, try to pour off as much solvent as
    possible without disturbing the crystals.

    15. Place crystals in a 1000 ml flask and dissolve in
    tetrahydrofurane.(Use only as much as absolutely necessary.) Label
    this solution "A".

    16. Slowly mix 200 ml. tetrahydrofurane and 20 grams lithium
    aluminum hydride in a 500 ml flask, and label it solution "B".
    (By the way, lithuim aluminum hydride ignites on contact with
    moisture. Protect eyes and hands.)

    17. Mix solutions "A" and "B" slowly, stirring constantly.

    18. Prepare a water bath and heat solution for three hours,
    stirring for four minutes every half hour. When not stirring, make
    sure to use aspirator tube.
    / / <--- Rubber Tubing
    \**{ }**/<---- One hole rubber stopper
    /**{ }**\ and glass tubing
    / { } \
    / { } \
    : :
    : :
    : :
    \ ~~~~~~~~~~~~~~~:_____________:~/

    Heat source

    Figure B.

    Place Figure B. flask at a higher level than Figure A. flask. Run
    tube from Figure B. flask down to left side of figure A. flask,
    replacing funnel with glass tubing. Disconnect right side tube
    from vacuum source. This will be used as the aspirator tube.

    19. When this is completed, allow the flask to remain at room
    temperature for about 20 minutes. Then place in salted ice bath,
    and cool to 0 degrees C. Add a small amount of chilled methanol,
    stirring gently until solution appears murky.

    20. Filter this murky solution through a paper filter in a funnel,
    and collect the filtered liquid in a flask.

    21. Add 100 ml. of tetrahydrofuran through the filter and collect
    in the same flask. Now heat the solution in a water bath until
    most of the tetrahydrofuran is evaporated and a gooey substance

    22. Place little piles of this substance on a cookie tray and dry
    with a heat lamp for three or four hours.

    Well, after all that you now have DMT. Was it worth it? To ingest,
    crumble a small quantity with parsley or mint, and smoke. Do not
    inject. Do not mix with tobacco.
  2. katukulysm

    katukulysm Mercury Member

    Reputation Points:
    Feb 14, 2005
    from U.S.A.
    sorry for the scramble in the topic above