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Morphine extraction: Save those veins extract the M

Discussion in 'Morphine' started by myfavoriteaccident88, Oct 20, 2007.

  1. myfavoriteaccident88

    myfavoriteaccident88

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    Everyone knows that injecting that shit in pills is dangerous and will cause lots of trouble. lose an arm or veins will shut down very quickly...

    Anyways here is a procedure that i originally posted in Newbies forum but i meant for it to be posted here. It is meant for 30mg Extended-release morphine sulphate pills. Some of which have beads, and some are just pills with a coating.

    This will get the pure morphine freebase while getting rid of all that other junk. This will make the morphine totally pure and very safe for injection.

    Since its freebase tho it would be advisable to turn it back into a salt right away. Or if u can keep it stored dry and safe then just dissolve it in vinegar before shooting.

    So heres a step by step easy as shit way.

    Supplies:

    -Mineral spirits
    -Toluene
    -Concentrated Ammonia or some other base
    -Muriatic Acid or some other acid
    -Pyrex bowl
    -Porcelain bowl
    -60 mL gardening syringe
    -Glasses
    -Graduated measuring cup
    -Paper coffee filters
    -hydrion pH papers
    -Heat source - If you want to do it professionally, then use a labratory heating element device listed in the elemental scientific catalogue. Right next to the magnetic stirring devices, which you might want as well. both items will cost you a total of $300. Otherwise this works as well -(outside with one of those camping stoves with an electric element would be the best, But if you must do it indoors and use your oven you better turn on the over head fan and pull a stool up next to your stove and be ready with the lid to the bowl just incase it flashes.)



    All of this stuff can be bought at hardware and gardening stores but if you can't manage to find Toluene because youre from the USA then use Xylene.

    1- Remove the pill coating from your 20 pills with a piece of tissue paper dampened with acetone, if you dont have acetone laying around your crib just use water.




    2-Crush up your 20 pills with shells removed and then place the powder in the pyrex casserole bowl. Make up a 50 mL solution of distilled water that is slighly acidic around pH 5 or 6. Add the Acidic Water to the powder and let them soak with no heat.

    3-Make up a solution (150 mL) of 80% mineral spirits and 20% toluene or the substitutions of the two. Add this solution to the Acidic water and stir vigirously for a few minutes.



    4-Be precise - use a themometer to moniter the inside temps. The temps stated on the dial do not heat the oven to the temperature listen on the dial. Turn the stove up to about 50 degrees celcius and leave it for ten minutes now turn it up to 80 degrees celcius and leave it for an additional 10 or fifteen minuites. During this time period stir the solution ever few minutes. Now tilt the bowl up and suck up with your syringe the entire 50 mL water solution (which is the bottom layer) and even 10 ml (in a seperate action) of the Nonpolar layer. Squirt out the Water layer into a clean pocelain bowl that can be heated on the stove, MAKE SURE you dont get any of the non polar into it.






    5-Add an additional 50 mL of acidic water to the pyrex bowl and do exactly the same thing as you did with the previous 50 mL. You're done with the non polar so you can put it away. Once you have the 100 mL of the morphine/water solution in the porcelain bowl put it on the stove and heat to 90 degrees celcius for 5 minutes. (Around halfway between low and the next notch up before medium on your stove) You should really use a labratory heating element. Now while its still piping hot pour it into a clean glass and funnel cup with cotton stuffed in the spout of the funnel. Pour in an extra 5 ml through the funnel to get an morphine thats trapped.



    6- Add Ammonia to the solution drop by drop until you hit a pH of 9.1. One you hit the 9.1 put the bowl in the freezer for 15 minutes stir it up then put it in the refridgerator for another 15 minutes. now pour the stuff into a funnel with 3 coffe filters in it, make sure to wet the filters with cold water before you pour in the mix. Once its filtered you will get the morphine freebase, if you wanna inject it as it is just mix it with some vinegar or dry it out and cook it with Acetic anhydride. So theres a walkthrough step by step, its not so bad, plus its better than wasting dope by trying to make it injectable with just water. Once you have this base cooking up heroin is even easier than this extraction. BTW this extraction on average yields about 95 percent of the total morphine from the pills.
     
    Last edited by a moderator: Dec 10, 2011
  2. Psych0naut

    Psych0naut Platinum Member

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    This is a perfect guide for people who want to extract morphine from their pills, but it was even better when the pictures of each step were still visible, could SWIY please upload them again, but to the forum this time? It would be highly appreciated cause it's one of the best extractions posted on D-F, mainly because of it's harm reducation value. It describes every step of the extraction very well and is of much use to many people.
     
    Last edited: Feb 1, 2008
  3. moda00

    moda00 R.I.P.

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    Question- what about the tiny little morphines that look a little like lsd microdots? Swim knows this isn't a pill id site, she knows what they are, but was surprised to find an opiate pill so tiny and withno markings at all.. They are labeled morphine sulphate soluble 10mgs on the container, have no markings, plain white and soft and bitter, and swim has only taken sublingual/oral as prescribed during and after a little incident lol, but wondering if these have fillers or if soluble morphine sulphate is injectable?? She has a bit of a needle fixation and is trying to behave herself on the heroin but has these babies left over and wants to do something fun with them! On the other hand she's never fukked with morphine with the exception of sniffing the brown 30s a couple times way back in the day, long before she started iv heroin and then subsequently quit and got on methadone.. not even sure if she'd enjoy/feel iv morphine in that dosage range with her tolerance, and doesn't want to screw up her opiate maintenance as she has only "relapsed" a few times in a little over two years and can't do the whole dope thing regularly anymore, too tedious and the rewards quite minimal.. but she's just having evil thoughts ;) Perhaps this belongs in a new thread, but swim just wanted to know if the above extraction is necessary and/or if it would work for this style of morphine pills? If one were to crush them she'd estimate the quantity of powder would be equivalent to the powder in one to three average shots of heroin (depends on size of course, but maybe about a gram's worth or less.. not a lot..) but she will not even consider trying to bang anything in pill form without knowing the safety and contents.. and would likely not inject a pill in general, and esp. not without doing such extraction/isolation of the safe/pure compound.. but she is just curious, as she's never seen such morphines.. thanks,
    edit: swim still has the morphs sitting around, lol, her opiate motivation is quite lacking.. she probably won't do anything with them.. but is still quite baffled at how they differ from most prescription painkillers produced commercially for pharma use.. weird..
     
    Last edited: Mar 23, 2008
  4. fnord

    fnord

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    There was pics missing from other threads,shoot alfa a message it could be a forum issue.
     
  5. raven3davis

    raven3davis R.I.P.

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    OP is banned but hypothetically what kinda of morphine pills would this work for? Are there any inactive ingredients in certain brands that need to be looked out for that will gakk the fuck up?
     
  6. radiometer

    radiometer bananadine addict

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    That'll teach 'em to upload their photos next time!
     
  7. Psych0naut

    Psych0naut Platinum Member

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    Just a small addition of info to the thread; once a person ends up with freebase morphine after following the procedure outlined by the OP, the best morphine salt to form would be the acetate. Here are the solubilities of the following morphine salts in water:

    - The freebase monohydrate has a solubility of 0.2mg/ml in water
    - The hydrochloride salt has a solubility of 50mg/ml in water
    - The sulphate salt has a solubility of 65mg/ml in water
    - The acetate trihydrate salt has a solubility of 445mg/ml in water

    To form the acetate salt from morphine freebase obtained after following the outlined morphine extraction, one simply has to put the collected morphine freebase in clear, white, distilled vinegar(which can be gotten from any medium sizer or large supermarket, and for less than 1 €/$/₤ or whatever) and it will inmediately dissolve. Use about 80-100ml of clear distilled household vinegar per gram of morphine base. Once the morphine base has completely dissolved and so turned into the acetate, the solution can be boiled down to obtain the morphine acetate for further purposes. Don't worry too much about heat destroying the morphine, morphine decomposes at 254°C, according to the Merck Index, the chemistry bible regarding chemical properties etc. If one uses clear white distilled vinegar, it won't contain any rubbish which would stay behind in the end product when boiling down the vinegar. Be shure that all the vinegar has evaporated by letting it dry for 5-10 more minutes after all the vinegar appears to be boiled off.
     
    Last edited: Mar 23, 2008
  8. travelingman

    travelingman

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    Does anyone know a way to attain morphine sulphate from Morhine HCl???
     
  9. moda00

    moda00 R.I.P.

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    I've seen people talk about doing Sulfate to Hcl.. but apparently sulfate is decently water soluble, more than hydrochloride- is there a specific reason swiy wants to convert this particular way? Depends what needs to be done I suppose. Maybe check the newbie chem forum, as I don't know much about chemistry..

    Material Safety Data Sheet (MSDS) got this:
    Morphine Sulfate, USP
    1g/15.5ml at 25 degrees C

    edit again, psych0naut posted this above, may be more applicable in mg's:

     
    Last edited: Apr 6, 2008
  10. Ididnotinhale

    Ididnotinhale

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    sorry if this answer has been inferred, but:

    Does this method work for the new extended release morphine that turn to jell?
    Also, if a random dog was to do this with 10 er pills, would that be to much material to inject?

    Thanks
     
  11. Psych0naut

    Psych0naut Platinum Member

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    SWIM has tried the procedure on MS Contins which gel up when they come in contact with water. Unfortunenately he used 7x30mg of Morphine, all he had left, and he ended up with around 30-40mg, which wasn't even completely clean. This method only works with normal MS Contins, or instant release morphine. Morphine can probaply be extracted from MS Contins which normally turn into gel, but it would be pretty complicated.
     
  12. man in the desert

    man in the desert Silver Member

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    Re: Morphine extraction: FOR THOSE WHO INJECT PILLS

    hi there: FOR THOSE WHO WANT TO INJECT MORPH PILLS :thumbsup:;)

    Just letting you all know that there is an easier way to extract morph from your pills than having to buy and build a labratory. The method is so simple and takes 5-10 mins with no chems just a simple prep method. This method stops all the shit from getting in your viens and is very safe. It also works perfectly as i have used this method for years with zero danger. But before i go through it i want to say the following.

    There is no need to go to such a dramatic measure for extraction in using all these instruments and methods. You end up losing product and time. YOU DO NOT NEED TO COOK THE PILLS IN A SPOON EITHER AS THIS FUCKS UP THE CHEMICLS AND THE WAXES IN THE PILLS. MORPHINE IS SOLUABLE IN WATER! THE WAXES ARE NOT!! DO NOT COOK A CRUSHED PILL ON A SPOON AS IF IT WAS HEROIN !!! the pills are professionally engineered in a lab, heroin is not.

    Anyway with that said now lets go onto EZ method.
    Depending on where you live it may be difficult to get good needle tips and filters. In australia we have these at needle exchanges so just ask for them. you pay have to pay $1 or two but thats it!

    you need:
    1. Your pick and barral for injection (obviously!) try to use a five ml barrel minimum 1mls a re useless. I use 10ml barrels as they fit more than enough.
    2. get some steriod tips as they are wider and draw the product up quicker.
    3. a small cup (pref a shot glass with a curved base.)
    4. a spoon and some paper.
    5. some wet towls (like the ones from fast food joints eg KFC.) you can also use swabs. these are usually included as part of your pick pack!
    and thats it!

    method.

    1. wipe the pill with the swab to get the surface paint off. you'll only need 1 or two, the shit comes straight off.

    2. lightly dry the pill/s (if you have 30ml pills use about 3 of 'em depending what your used to) i usually use 60ml or 100ml tabs.

    3. put the pills in some paper folded in half. tap a desert spoon gently over them to crush them up. Then use the curved part of the spoon to roll over the broken bits. It doesn't have to be total powder so don't be too fussy.

    4 pour the crushed tabs into the shot glass and add about 8ml-10ml of clean sterilised water and use the cover tip of the pick or some other clean object as a stirer and stir for a about a minute. you can crush the powder more if you want during this time.

    5. Let sit for about 5 min (i usually have a shower) When you come back the un-important shit will be sitting on the bottom. this is all the waxes etc. If you want you can give another brief stir and let sit for a min or 2.

    6. attach the filter to the barrel (without the pick) and attach the steroid needle tip to the other side of the filter and carefully draw up the water. If you don't have or can get a filter use a cigerette butt and break it up a bit and draw thru that! be carefull not to get the tip into the powder at the bottom as the needle tip can get blocked and its a pain in the arse to clean it midway. the filter will stop the shit but if using a cig butt there may be more shit picked up.

    7. take off the filter attach your tip and you're done.

    ps add some water to the remaining powder as there is still some more morph in there and you can have a second blast or save it for later, but it won't be as strong. its just to keep you up iof you have to go to work etc.
    Hope this helped!

    pps be sure to always clean the injection site with a swab! dirt on the arm is the main reason people get absesses and so on.:vibes::) ALSO, PLEASE PASS THIS METHOD ON TO ALL WHO ENGAGE IN SUCH DANGEROUS HABITS, ITS EASIER AND SAFER THAT PLAYING LAB TECH
     
  13. runfrom MURDER

    runfrom MURDER Silver Member

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    Re: Morphine extraction: FOR THOSE WHO INJECT PILLS

    SWIM tried your method today, mostly.

    He only did it with one 15mg IR Morphine pill though, and had to use more water than what was said. SWIM had to of shot up at least 5 times, leaving him with lots of bumps. This was SWIM's first time ever shooting up.

    There was no high at all. SWIM thinks the morphine got diluted from too much water? SWIM needed the extra water so that he wouldn't get the binder / filler crap in his needle.

    Edit: One of the places that SWIM shot up at is now a huge bump. Uh oh?!... :(
    Edit 2: Next morning, SWIM's arms are fine. Little pain when touched, but the bumps are gone. :)
     
    Last edited: May 30, 2008
  14. Junkiebaddypowder

    Junkiebaddypowder Silver Member

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    swim has done this many times. its not the safest nor the best way but swim thinks it works just fine and meets goal in mind. The very hardest part is to remember what to do with each different generic. Swim has found that some require one procedure while the exact same pill and mg of a differnt manufacturer reqiure a different routine.


    Say swim had a 60mg er ms contin the brand is endo pharm which is swims favorite of all. The pill is a long oval shaped pill thats peach colored like the .5 mg xanax footballs. The pill has 60 written on one side and e655 on the other side..

    this is the prcoedure that swim uses and had sucess with for that specific pill. mind swiy that this is basic procedure for a quick rush not the long drawn out safe way. swim recommends the safe way any day but dosnt have to time patience or knowledge to properly carry it out. swim also realizes that it pays many consequences for taking the shortcut.. so
    take the pill and crush it a fine powder and put it in spoon. Add water ( the amount depends on whether swiy wants one dose of it all or wants to dilute it a little more and get another load. for 1 rig full use between 1.5 -2 ml)

    stir it up and it will turn to a clumpy gel. heat it untill the jel starts to turn a pale version or its original color. as it is heated evenly the gel will turn in to a rubbery blanket while underneath will be liquid. do NOT stir. use a clean needle cap to slide the film all to one side of the spoon so it is easier to get to the liquid. strain it thorugh a cotton into a rig while it is still hot. ( the longer it sits in the spoon with the film the less liquid there will be becuase they will start binding again as it cools off and it will turn right back in to a nonfunctional gel. so make sure to suck it in the rig while its still hott. Make sure to let it cool to room temp before attempting anything with it. ( so that is the shitty unhealthy way but its fast and easy, but remmeber it will contain wax and other things that will harm a human body so its always a good idea to take the time to learn the other ways)

    one more thing. swim has found that swiy can take the film leftover in the spoon ( removing the cotton first ) and push it backto the middle and add 1 ml of water to it and repeat the above process. granted it will not be as strong and powerful as the first but its still something worth having and will always get swiy off unless tolerance is extremely high.


    hope this could be of assistance
     
  15. BumpBump

    BumpBump Silver Member

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    swim wonders if its so easy to extract morphine from a pill with loads of binders, why is it not easy to extract it from poppy tea lol.
    Swim is gonna try this with some otc morphine products that have been dried out and then rehydrated.
     
  16. man in the desert

    man in the desert Silver Member

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    To runfrmmurder:
    the reason he had big lumps could be a few reasons,
    1.he went thru the vien and into the tissue,
    2. he applied to much pressure to quickly and did not loose the turnequette properly.

    i have done that from time to time, no biggy but it does freak you out the first time which is not what you want, hate that panick.
    You only need a little water 6-ml for any tablet. the water may weaken it a little but its the strength of the pill u use that makes a difference. also what size pick did you use? a 10ml barrel is more than enuff to take 8 mls of solution. you don't want the pasty shit just the water, thats why swim should use an injection filter, they stop the shit from going in and you get a nice solution. If you follow the instructions with the right equip i mention you can't go wrong. just becareful with any pill that is half the drug and half some other shit.

    Junkie baddypoweder,

    sounds like a lota fucking around! and like i said you don't cook a engineered product you only have to disolve it in 6-8m water with a 10ml barrel. but if that works for you then fine. what kinda filter do you use? your solution must be pretty milky.

    Bumpbump
    if you reduce your tea right down to a small amount, it turns cluggy add some alcohol, use a filter and go for it. be sure to rinse the sides of the pot to get all the opium you can then reduce it some more and don't burn the rpoduct. that should work.

    Are you're talking about liquid otc morph products? such as?
     
  17. BumpBump

    BumpBump Silver Member

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    yeh j collis brownes mixture 1mg morphine to 5ml
     
  18. man in the desert

    man in the desert Silver Member

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    wow, there's nothin down in oz like that!
    cheers man.
     
  19. power plunger

    power plunger

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    Best not to destroy your veins and heart by IV-ing pills. If you want to inject something stick to smack. I just got a box of Endone (Oxycodone) 5mg, there is 20 pills to a box.
    So i crushed all the pills up in pestle added 10ml of cold water, this stuff dissolves almost instantly. I then shot 5ml into my mouth and the other 5ml into my ass. That was a few hours ago and i havnt stopped noddin off since. Hardly get off on the street heroin these days so im happy with this so far.
     
  20. sirdrugalot

    sirdrugalot

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    would the first chemical extraction at the top of the page work for extracting 120mg DHC continus also?
    can dihydrocodeine with stand higher temps than codeine?
    is it safe to iv dihydrocodeine or will make you turn into mr. blooby and die like codeine will?
    sorry about all the questions but swim cant find much info dihydro iv, is it worth shooting?